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Sulfuryl chloride fluoride

SO2F2 ClSO2(NCO) SO2BrF

Sulfuryl chloride fluoride is a chemical compound with the formula . It is a colorless, easily condensed gas. It is a tetrahedral molecule.

Liquified sulfuryl chloride fluoride is employed as a solvent for highly oxidizing compounds.

Preparation

The laboratory-scale synthesis begins with the preparation of potassium fluorosulfite: : This salt is then chlorinated to give sulfuryl chloride fluoride : Further heating (180 °C) of potassium fluorosulfite with the sulfuryl chloride fluoride gives sulfuryl fluoride. :

Alternatively, sulfuryl chloride fluoride can be prepared without using gases as starting materials by treating sulfuryl chloride with ammonium fluoride or potassium fluoride in trifluoroacetic acid. :

References

References

  1. (2007). "Syntheses, Solution Multi-NMR Characterization, and Reactivities of [C6F5Xe]+Salts of Weakly Coordinating Borate Anions, [BY4]-(Y = CF3, C6F5, CN, or OTeF5)". Inorganic Chemistry.
  2. Seel, F.. (1967). "Inorganic Syntheses". [[Inorg. Synth.]].
  3. Seel, F.. (1967). "Inorganic Syntheses". [[Inorg. Synth.]].
  4. (1992). "A Convenient Preparation of Sulfuryl Chloride Fluoride". Journal of Fluorine Chemistry.
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sulfuryl-compounds oxyfluorides oxychlorides sulfur-oxohalides nonmetal-halides inorganic-solvents
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