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4-Hydroxyphenylglycine


Column 1Column 2
4-Hydroxyphenylglycine (HPG). (R)-D-HPG shown on left; (S)-L-HPG shown on right.
IUPAC name
Nortyrosine
Systematic IUPAC name
Amino(4-hydroxyphenyl)acetic acid
Other names
3-Amino-2,3,6-trideoxy-3-methyl-L-lyxo-hexopyranose
CAS Number.mw-parser-output .plainlist ol,.mw-parser-output .plainlist ul{line-height:inherit;list-style:none;margin:0;padding:0}.mw-parser-output .plainlist ol li,.mw-parser-output .plainlist ul li{margin-bottom:0}37784-25-1
3D model (JSmol)Interactive image
Beilstein Reference513130
ChEBICHEBI:50418CHEBI:15695 D
ChEMBLChEMBL130865
ChemSpider83189
ECHA InfoCard100.012.139
EC Number213-353-2
KEGGC03493 D
PubChem CID92143
UNII7UYG7X0F53
CompTox Dashboard (EPA)DTXSID90860473
InChI
Key: LJCWONGJFPCTTL-UHFFFAOYSA-N
SMILES
C1=CC(=CC=C1C(C(=O)O)N)O
Chemical formulaC8H9NO3
Molar mass167.164 g·mol−1
Except where otherwise noted, data are given for materials in their standard state (at 25 °C [77 °F], 100 kPa).

Infobox references | |

4-Hydroxyphenylglycine (HPG) is a non-proteogenic amino acid found in vancomycin and related glycopeptides. HPG is synthesized from the shikimic acid pathway and requires four enzymes to synthesize: Both L- and D-HPG are used in the vancomycin class of antibiotics. Tyrosine, a similar amino acid, differs by a methylene group (CH2) between the aromatic ring and the alpha carbon.

Biosynthesis of HPG

HPG is synthesized from prephenate, an intermediate in the shikimic acid pathway and also a precursor to tyrosine. Prephenate is aromatized by prephenate dehydrogenase (Pdh) using NAD+ as a cofactor to produce 4-hydroxyphenylpyruvate. 4-Hydroxyphenylpyruvate is then oxidized by 4-hydroxymandelate synthase (4HmaS) using oxygen to form 4-hydroxymandelate and hydrogen peroxide. 4HmaS is a non-heme iron-dependent dioxygenase. The reaction mechanism of this unique oxidation was proposed by Choroba et al in 2000

Proposed mechanism by Choroba et al for the oxidation of 4-hydroxymandelate.

4-Hydroxymandelate is subsequently oxidized by hydroxymandelate oxidase (Hmo) to 4-hydroxylbenzoylformate, using FMN as a cofactor. Finally, 4-hydroxyphenylglycine transaminase (HpgT) transfers an ammonia moiety from a donor to 4-hydroxylbenzoylformate to form HPG. Several different molecules can serve as the nitrogen donor for the transamination, however, Hubbard et al suspect L-tyrosine to serve as the most efficient donor. By doing so, the following cycle is constructed:

HPG synthetic cycle

HPG is also synthesized in Herpetosiphon aurantiacus using enzymes Haur_(1871,1887,1888).

  • Vancomycin
  • Oritavancin
  • Glycopeptide antibiotics
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