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4-ANPP


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Preferred IUPAC name
N-Phenyl-1-(2-phenylethyl)piperidin-4-amine
Other names
desproprionyl fentanyl; 4-anilino-N-phenethylpiperidine; 4-ANPP; ANPP
CAS Number.mw-parser-output .plainlist ol,.mw-parser-output .plainlist ul{line-height:inherit;list-style:none;margin:0;padding:0}.mw-parser-output .plainlist ol li,.mw-parser-output .plainlist ul li{margin-bottom:0}21409-26-7
3D model (JSmol)Interactive image
AbbreviationsANPP
ChemSpider87058 Y
ECHA InfoCard100.169.974
EC Number642-161-5
PubChem CID88890
UNIIQ88EHD0U8G
CompTox Dashboard (EPA)DTXSID40175680
InChI
InChI=1S/C19H24N2/c1-3-7-17(8-4-1)11-14-21-15-12-19(13-16-21)20-18-9-5-2-6-10-18/h1-10,19-20H,11-16H2Key: ZCMDXDQUYIWEKB-UHFFFAOYSA-N
SMILES
C1CN(CCC1NC2=CC=CC=C2)CCC3=CC=CC=C3
Chemical formulaC19H24N2
Molar mass280.415 g·mol−1
Legal statusAU: S9 (Prohibited substance)
BR: Class D1 (Drug precursors)
UK: Scheduled Precursor
US: Schedule II
UN: International Red List
Except where otherwise noted, data are given for materials in their standard state (at 25 °C [77 °F], 100 kPa).

Infobox references | |

4-ANPP, also known as 4-anilino-N-phenethylpiperidine (4-ANPP), 4-aminophenyl-1-phenethylpiperidine, or despropionyl fentanyl, is a direct precursor to fentanyl and acetylfentanyl. It is commonly found as a contaminant in samples of drugs containing fentanyl, which may include samples represented by the supplier as heroin or other opioids. It is not psychoactive and is present only as a result of improper chemical purification.

4-ANPP is useful in the synthesis of pharmaceuticals, primarily fentanyl and related analogs. Paul Janssen (founder of Janssen Pharmaceutica) first synthesized fentanyl in 1960 using a similar method, with Benzylfentanyl as an intermediate. The following synthesis, developed by an individual under the pseudonym of Siegfried, involves the reductive amination of N-phenethyl-4-piperidinone (NPP) with aniline to make to 4-ANPP. This product is reacted with propionyl chloride or acetyl chloride to form either fentanyl or acetylfentanyl.

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